Table 4.
DRS studies: temperatures of the relaxation processes
Compositions |
Relaxation temperatures (ω = 1 Hz) |
||||
---|---|---|---|---|---|
Reactivity (R) | MDI (%) | PIC (%) | Tr0 (°C) | Tr1 (°C) | Tr2 (°C) |
0.04 |
100 |
0 |
−98 |
−60 |
- |
0.06 |
90 |
10 |
−96 |
−54 |
- |
0.1 |
80 |
20 |
−91 |
−52 |
41 |
0.14 |
65 |
35 |
−90 |
−51 |
59 |
0.18 |
50 |
50 |
−89 |
−56 |
70 |
0.22 |
35 |
65 |
−88 |
−65 |
98 |
0.26 | 20 | 80 | −87 | −76 | 108 |
Compositions and glass transition temperatures of OIS obtained from DRS investigations at frequency ω = 1 Hz, depending on the reactivity R of the organic component of OIS.