Table 2. 1H and 13C NMR Data of Compounds 3 and 4 in CD3CN-d3.
3 |
4 |
|||
---|---|---|---|---|
no. | δC | δH (J in Hz) | δC | δH (J in Hz) |
1 | 167.6 C | 167.6 C | ||
2 | 104.8 C | 104.8 C | ||
3 | 148.8 C | 148.9 C | ||
4 | 142.8 C | 142.2 C | ||
5 | 137.9 C | 137.6 C | ||
6 | 116.7 CH | 6.89 s | 117.5 CH | 6.87 s |
7 | 129.9 C | 129.9 C | ||
8 | 104.6 CH | 6.45 s | 104.9 CH | 6.45 s |
9 | 152.4 C | 152.2 C | ||
10 | 19.1 CH3 | 2.28 s | 19.9 CH3 | 2.27 s |
11 | 26.8 CH2 | 3.07 t (7.6) | 28.8 CH2 | 3.05 t (7.6) |
12 | 33.2 CH2 | 2.71 t (7.6) | 33.8 CH2 | 2.72 t (7.6) |
13 | 173.9 C | 173.1 C | ||
13-OMe | 52.4 CH3 | 3.66 s |