. Author manuscript; available in PMC: 2015 May 1.

Published in final edited form as: J Pharm Sci. 2014 Mar 12;103(5):1356–1366. doi: 10.1002/jps.23926

Table 1.

T_g (onset) temperatures measured by DSC, previously reported ln(τ^β, h) measured by thermal activity monitor²⁸ and previously reported <u2>⁻¹ measured by neutron scattering²⁹ for lyophilized formulations (without protein) prepared using the standard freeze-drying cycle.

	T_g (onset) (°C) ± SD	ln(τ^β, h) (at 323K)	<u²>⁻¹ (Å⁻²)±SD (at 323K)
5% HES	203±3	3.4	2.25±0.04
5% Trehalose	98±2	2.0	9.10±0.50
5% Sucrose	64±2	0.2	6.72±0.17