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. 2014 May 13;12(5):2802–2815. doi: 10.3390/md12052802

Table 2.

13C NMR shifts of korormicins G–K (26).

No. Korormicin
G (2) H (3) I (4) I (4) J (5) K (6)
δC, mult. a δC, mult. b δC, mult. b δC, mult. a δC, mult. a δC, mult. a
1 - - - - - -
2 174.7, qC 168.5, qC 168.5, qC 168.5, qC nd c 174.3, qC
3 50.0, CH 125.0, qC 125.0, qC 125.0, qC 50.0, CH 50.4, CH
4 39.9, CH2 133.7, CH 134.0, CH 134.0, CH 40.0, CH2 40.4, CH2
5 85.8, qC 87.2, qC 87.2, qC 87.2, qC nd c 85.6, qC
6 32.4, CH2 31.2, CH2 31.1, CH2 34.6, CH2 32.9, CH2 32.8, CH2
7 8.2, CH3 8.0, CH3 8.0, CH3 8.1, CH3 8.3, CH3 8.4, CH3
8 25.9, CH3 23.9, CH3 24.1, CH3 24.2, CH3 25.9, CH3 26.2, CH3
NH - - - - - -
1′ 172.0, qC 170.1, qC 170.2, qC 170.2, qC nd c 171.7, qC
2′ 42.3, CH2 43.9, CH2 44.0, CH2 43.1, CH2 42.7, CH2 42.7, CH2
3′ 64.7, CH 63.5, CH 63.8, CH 64.6, CH 64.8, CH 65.0, CH
OH - - - - - -
4′ 129.3 CH 132.8 CH 132.2 CH 129.4, CH 127.6, CH 129.0 CH
5′ 130.0, CH 128.2, CH 128.5, CH 130.7, CH 130.6, CH 131.0, CH
6′ 126.4, CH 127.8, CH 127.4, CH 127.4, CH 124.0, CH 124.7, CH
7′ 132.0, CH 131.9, CH 132.5, CH 132.7, CH 136.6, CH 136.4, CH
8′ 31.1, CH2 37.2, CH2 37.1, CH2 38.2, CH2 30.5, CH2 30.6, CH2
9′ 55.3, CH 67.0, CH 72.1, CH 73.1, CH 128.3, CH 126.1, CH
OH - - - - - -
10′ 56.6, CH 71.4, CH 67.7, CH 68.0, CH 129.2 CH 131.4, CH
11′ 27.3, CH2 33.3, CH2 33.7, CH2 31.9, CH2 27.0, CH2 27.2, CH2
12′ 29.1 d, CH2 25.4, CH2 26.3, CH2 26.0, CH2 25.4, CH2 29.1 d, CH2
13′ 29.1 d, CH2 29.0 d, CH2 28.8 d, CH2 28.8 d, CH2 29.0 d, CH2 29.1 d, CH2
14′ 29.1 d, CH2 29.0 d, CH2 28.6 d, CH2 28.58 d, CH2 28.6 d, CH2 29.1 d, CH2
15′ 29.1 d, CH2 29.0, CH2 28.6 d, CH2 28.55 d, CH2 31.4, CH2 29.1 d, CH2
16′ 31.6, CH2 31.3, CH2 31.2, CH2 31.7, CH2 22.0, CH2 31.6, CH2
17′ 22.6, CH2 22.1, CH2 22.1, CH2 22.6, CH2 13.5, CH3 22.6, CH2
18′ 13.9, CH3 13.9, CH3 13.9, CH3 13.9, CH3 - 14.1, CH3

a CDCl3; b DMSO-d6; c No HMBC data was recorded for the qC due to low yield of 5, these carbons remain unassigned; d interchangeable.