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. 2014 Feb 28;1(Pt 2):110–118. doi: 10.1107/S2052252514002838

Table 4. Unit-cell parameters of 1 at different temperatures.

    10 K 35 K 70 K 100 K
Single-crystal measurement a (Å) 11.0104 (3) 10.9784 (14) 11.0470 (12) 11.030 (2)
b (Å) 10.0398 (2) 10.0056 (13) 10.1293 (11) 10.092 (2)
c (Å) 18.6040 (4) 18.488 (3) 18.652 (2) 18.637 (3)
β (°) 97.320 (2) 97.223 (4) 97.223 (3) 97.24 (2)
Powder diffraction a (Å) 11.0595 11.0491 11.0532
b (Å) 10.1355 10.1156 10.1303
c (Å) 18.6883 18.6742 18.6769
β (°) 97.191 97.223 97.175