Table 4. Unit-cell parameters of 1 at different temperatures.
| 10 K | 35 K | 70 K | 100 K | ||
|---|---|---|---|---|---|
| Single-crystal measurement | a (Å) | 11.0104 (3) | 10.9784 (14) | 11.0470 (12) | 11.030 (2) |
| b (Å) | 10.0398 (2) | 10.0056 (13) | 10.1293 (11) | 10.092 (2) | |
| c (Å) | 18.6040 (4) | 18.488 (3) | 18.652 (2) | 18.637 (3) | |
| β (°) | 97.320 (2) | 97.223 (4) | 97.223 (3) | 97.24 (2) | |
| Powder diffraction | a (Å) | – | 11.0595 | 11.0491 | 11.0532 |
| b (Å) | 10.1355 | 10.1156 | 10.1303 | ||
| c (Å) | 18.6883 | 18.6742 | 18.6769 | ||
| β (°) | 97.191 | 97.223 | 97.175 |