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. Author manuscript; available in PMC: 2015 Feb 1.
Published in final edited form as: Phytochem Lett. 2013 Dec 4;7:130–132. doi: 10.1016/j.phytol.2013.11.001

Table 1.

1H (500 MHz) and 13C NMR (125 MHz) spectral data for 1 in CD3OD.

Position Miconioside C (1)

δ c δ h δ c δ h
Aglycone Glc
2 80.2 5.47 dd (3.0, 12.9) 1″ 105.3 4.69 d (7.7)
3 44.5 2.85 dd (3.0, 17.0)
3.15 dd (12.9, 17.0)
2″ 75.7 3.51 t br (8.7)
4 199.5 3″ 78.0 3.41 t (8.5)
5 159.9 4″ 71.7 3.25-3.35*
6 113.2 5″ 77.1 3.25-3.35*
7 162.7 6″ 68.6 3.60 dd (5.6, 11.2)
3.84 dd (1.7, 11.2)
8 112.0 Api
9 159.0 1‴ 110.9 4.89 d (2.0)
10 106.4 2‴ 77.9 3.80 d (2.0)
1′ 140.6 3‴ 80.5
2′, 6′ 127.2 7.53 d (7.2) 4‴ 74.9 3.67 d (9.6)
3.74 d (9.6)
3′, 5′ 129.7 7.42 t (7.2) 5‴ 65.9 3.49 d (3.1)
4' 129.5 7.35 t (7.2)
6-Me 9.8 2.14 s br
8-Me 9.2 2.14 s br
*

overlapped signals.