Table 4.
Serum Interday Analysis Results (ng element/mL sample)
| Sample | Average | Caa | Ka | Mga | Naa | Cr | Mn | Fe | Co | Cu | Zn | Se | Mo |
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| 1 | Day 1 | 93.7 | 217 | 15.2 | 2430 | NDb | 1.14 | 74.1 | 0.238 | 1420 | 721 | 107 | 3.05 |
| Day 2 | 93.4 | 213 | 14.8 | 2070 | 3.06 | 2.07 | 424 | 0.329 | 1430 | 768 | 105 | 4.41 | |
| Day 3 | 95.3 | 214 | 14.8 | 2340 | 4.27 | 2.38 | 615 | 0.160 | 1400 | 781 | 116 | 3.38 | |
|
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| Average | 94.2 | 215 | 14.9 | 2280 | 3.66 | 1.86 | 371 | 0.242 | 1417 | 757 | 109 | 3.61 | |
| %RSD | 0.872 | 0.729 | 1.37 | 6.71 | 23.4 | 28.2 | 60.4 | 28.4 | 0.882 | 3.43 | 4.63 | 16.0 | |
|
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| 2 | Day 1 | 92.9 | 206 | 17.4 | 2510 | ND | 2.02 | 242 | 0.198 | 985 | 724 | 114 | 1.04 |
| Day 2 | 92.0 | 202 | 17.5 | 2250 | 2.74 | 2.04 | 577 | 0.149 | 969 | 716 | 118 | 1.89 | |
| Day 3 | 91.5 | 194 | 16.7 | 2220 | 1.75 | ND | 2330 | 0.120 | 917 | 723 | 128 | 0.714 | |
|
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| Average | 92.1 | 200 | 17.2 | 2327 | 2.24 | 2.03 | 1049 | 0.156 | 957 | 721 | 120 | 1.21 | |
| %RSD | 0.635 | 2.36 | 1.93 | 5.60 | 31.2 | 0.515 | 87.3 | 20.7 | 3.01 | 0.45 | 4.54 | 40.8 | |
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| 3 | Day 1 | 93.2 | 238 | 18.8 | 2570 | ND | 0.803 | 353 | 0.251 | 972 | 779 | 119 | 1.32 |
| Day 2 | 94.8 | 237 | 18.9 | 2350 | 1.98 | 1.08 | 298 | 0.469 | 970 | 776 | 118 | 2.88 | |
| Day 3 | 92.1 | 223 | 17.7 | 2350 | 3.63 | ND | 16.9 | ND | 927 | 761 | 133 | 0.554 | |
|
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| Average | 93.3 | 233 | 18.5 | 2423 | 2.80 | 0.940 | 223 | 0.360 | 956 | 772 | 123 | 1.58 | |
| %RSD | 1.20 | 2.99 | 2.80 | 4.29 | 41.7 | 14.6 | 66.1 | 30.2 | 2.16 | 1.05 | 5.35 | 61.0 | |
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| 4 | Day 1 | 98.3 | 228 | 17.7 | 2440 | ND | 2.12 | 760 | 0.251 | 887 | 892 | 134 | 1.01 |
| Day 2 | 96.1 | 218 | 17.8 | 2320 | 3.78 | 3.44 | 1080 | 0.749 | 900 | 926 | 141 | 4.08 | |
| Day 3 | 93.7 | 206 | 16.4 | 2240 | ND | 44.0 | 2230 | 0.480 | 834 | 921 | 142 | 1.15 | |
|
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| Average | 96.0 | 217 | 17.3 | 2333 | 3.78 | 16.5 | 1357 | 0.493 | 873 | 913 | 139 | 2.08 | |
| %RSD | 1.94 | 4.24 | 3.56 | 3.52 | NA | 118 | 46.5 | 41.2 | 3.26 | 1.63 | 2.68 | 67.9 | |
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| 5 | Day 1 | 97.4 | 231 | 22.1 | 2610 | 2.77 | 1.26 | 520 | 0.291 | 1090 | 705 | 123 | 0.918 |
| Day 2 | 95.8 | 221 | 21.9 | 2300 | 5.81 | 1.73 | 292 | 1.32 | 1100 | 680 | 123 | 2.34 | |
| Day 3 | 96.0 | 211 | 21.2 | 2370 | 1.55 | ND | 448 | ND | 1030 | 713 | 129 | ND | |
|
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| Average | 96.4 | 221 | 21.7 | 2460 | 3.38 | 1.50 | 420 | 0.805 | 1073 | 699 | 125 | 1.63 | |
| %RSD | 0.736 | 3.70 | 1.85 | 5.40 | 53.1 | 15.6 | 22.7 | 63.8 | 2.87 | 2.00 | 2.28 | 61.84 | |
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| 6 | Day 1 | 98.3 | 225 | 20.6 | 2680 | ND | 2.14 | 857 | 0.291 | 1040 | 734 | 126 | 1.40 |
| Day 2 | 98.9 | 220 | 20.9 | 2220 | 2.77 | 6.22 | 460 | 0.311 | 1040 | 642 | 124 | 2.41 | |
| Day 3 | 89.9 | 190 | 18.5 | 2280 | 4.23 | 9.44 | 738 | 0.300 | 941 | 682 | 126 | 1.61 | |
|
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| Average | 95.7 | 212 | 20.0 | 2393 | 3.50 | 5.93 | 685 | 0.301 | 1007 | 686 | 125 | 1.81 | |
| %RSD | 4.27 | 7.35 | 5.47 | 8.53 | 29.4 | 50.3 | 24.2 | 2.72 | 4.63 | 5.49 | 0.79 | 24.1 | |
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| 7 | Day 1 | 89.8 | 212 | 20.2 | 2540 | ND | 0.903 | 410 | 0.758 | 1330 | 558 | 125 | 1.19 |
| Day 2 | 90.4 | 209 | 20.6 | 2090 | 3.01 | 15.8 | 736 | 1.69 | 1230 | 580 | 124 | 1.32 | |
| Day 3 | 91.4 | 205 | 20.0 | 2420 | 3.43 | 10.0 | 640 | 0.480 | 1250 | 558 | 124 | 1.37 | |
|
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| Average | 90.5 | 209 | 20.2 | 2320 | 3.22 | 8.91 | 596 | 0.976 | 1270 | 565 | 124 | 1.29 | |
| %RSD | 0.724 | 1.49 | 1.20 | 8.20 | 9.16 | 68.9 | 23.0 | 53.0 | 3.40 | 1.85 | 0.44 | 5.73 | |
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| 8 | Day 1 | 89.7 | 211 | 17.5 | 2440 | 3.39 | 0.743 | 317 | 0.131 | 1280 | 697 | 103 | 1.60 |
| Day 2 | 93.0 | 210 | 18.2 | 2020 | ND | 1.74 | 561 | 0.349 | 1160 | 659 | 110 | 1.33 | |
| Day 3 | 96.4 | 216 | 18.5 | 2460 | ND | 8.46 | 357 | 0.200 | 1240 | 684 | 112 | 2.17 | |
|
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| Average | 93.0 | 212 | 18.0 | 2307 | 3.39 | 3.65 | 412 | 0.227 | 1227 | 680 | 108 | 1.70 | |
| %RSD | 2.92 | 1.12 | 2.37 | 8.80 | NA | 94.0 | 25.9 | 40.0 | 4.07 | 2.31 | 3.33 | 20.7 | |
|
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| 9 | Day 1 | 100 | 230 | 17.9 | 2700 | ND | 12.7 | 4040 | 0.131 | 1260 | 799 | 137 | 1.86 |
| Day 2 | 96.7 | 213 | 17.4 | 2220 | 2.86 | 1.84 | 1270 | 0.189 | 1210 | 810 | 137 | 1.61 | |
| Day 3 | 95.5 | 211 | 16.8 | 2450 | ND | ND | 768 | 0.360 | 1180 | 815 | 149 | 2.23 | |
|
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| Average | 97.3 | 218 | 17.4 | 2457 | 2.86 | 7.27 | 2026 | 0.227 | 1217 | 808 | 141 | 1.90 | |
| %RSD | 1.89 | 3.91 | 2.49 | 7.98 | NA | 74.6 | 71.0 | 42.8 | 2.71 | 0.83 | 3.90 | 13.5 | |
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| 10 | Day 1 | 95.6 | 236 | 13.2 | 2510 | 14.2 | 3.66 | 546 | 0.318 | 1380 | 632 | 128 | 1.73 |
| Day 2 | 92.2 | 219 | 12.7 | 1970 | 1.50 | 1.74 | 815 | 0.709 | 1320 | 631 | 129 | 2.02 | |
| Day 3 | 96.3 | 228 | 13.0 | 2380 | ND | 7.02 | 655 | 0.240 | 1340 | 653 | 139 | 1.46 | |
|
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| Average | 94.7 | 227 | 13.0 | 2287 | 7.83 | 4.14 | 672 | 0.422 | 1346 | 639 | 132 | 1.74 | |
| %RSD | 1.86 | 3.07 | 1.37 | 10.1 | 114 | 52.71 | 16.4 | 48.5 | 1.84 | 1.58 | 3.99 | 13.2 | |
|
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| Pool | Day 1 | 95.4 | 222 | 17.5 | 2500 | 3.17 | 1.98 | 1930 | 0.411 | 1170 | 740 | 127 | 1.54 |
| Day 2 | 96.3 | 220 | 18.5 | 2170 | ND | 45.8 | 1710 | 0.509 | 1190 | 757 | 127 | 2.01 | |
| Day 3 | 97.5 | 229 | 18.1 | 2560 | 2.51 | 24.3 | 1410 | 1.54 | 1120 | 724 | 137 | 2.21 | |
|
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| Average | 96.4 | 224 | 18.0 | 2410 | 2.84 | 24.0 | 1683 | 0.820 | 1160 | 740 | 130 | 1.92 | |
| %RSD | 0.897 | 1.72 | 2.42 | 7.12 | 16.5 | 74.4 | 12.7 | 62.3 | 2.53 | 1.79 | 3.49 | 14.5 | |
|
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| Average | 94.3 | 217 | 17.8 | 2360 | 3.67 | 5.27 | 781 | 0.421 | 1134 | 724 | 125 | 1.86 | |
| % Diff from pool | −2.12 | −3.25 | −1.09 | −2.06 | 29.1 | −78.1 | −53.6 | −48.7 | −2.20 | −2.19 | −4.30 | −3.34 | |
Values reported in units of μg/mL
Values were not found to be greater than the IDL (Table 3)