Table 5.
Whole Blood Interday Analysis Results (ng element/mL sample)
| Sample | Average | Caa | Ka | Mga | Naa | Cr | Mn | Fea | Co | Cu | Zn | Se | Mo |
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| 1 | Day 1 | 60.1 | 1720 | 28.7 | 1590 | NDb | 15.6 | 500 | 0.507 | 950 | 7627 | 211 | ND |
| Day 2 | 59.8 | 1790 | 30.2 | 1730 | 2.33 | 18.2 | 491 | 0.543 | 953 | 8372 | 211 | 2.38 | |
| Day 3 | 62.1 | 1650 | 28.5 | 1710 | ND | 12.4 | 493 | 0.523 | 976 | 8828 | 225 | 1.63 | |
|
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| Average | 60.7 | 1720 | 29.1 | 1677 | 2.33 | 15.4 | 495 | 0.525 | 959 | 8276 | 216 | 2.01 | |
| %RSD | 1.69 | 3.31 | 2.55 | 3.69 | NA | 15.4 | 0.805 | 4.88 | 1.22 | 5.98 | 3.07 | 26.7 | |
|
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| 2 | Day 1 | 66.1 | 2010 | 35.8 | 1530 | 1.70 | 27.8 | 494 | 0.700 | 1022 | 6493 | 204 | 1.09 |
| Day 2 | 58.6 | 2040 | 35.1 | 1580 | 1.41 | 61.3 | 476 | 0.823 | 1060 | 6574 | 204 | 1.74 | |
| Day 3 | 61.3 | 1840 | 33.4 | 1460 | ND | 48.3 | 476 | 0.669 | 1010 | 6676 | 215 | 1.30 | |
|
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| Average | 62.0 | 1963 | 34.7 | 1523 | 1.56 | 38.0 | 482 | 0.761 | 1031 | 6581 | 208 | 1.52 | |
| %RSD | 4.99 | 4.49 | 2.86 | 3.22 | 13.1 | 44.4 | 1.77 | 11.4 | 2.08 | 1.14 | 2.56 | 20.7 | |
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| 3 | Day 1 | 65.9 | 1860 | 40.8 | 1680 | ND | 16.8 | 511 | 0.567 | 1039 | 5945 | 163 | 1.29 |
| Day 2 | 58.2 | 1850 | 39.0 | 1590 | 0.491 | 15.7 | 474 | 0.410 | 1005 | 6419 | 169 | 1.78 | |
| Day 3 | 59.9 | 1690 | 36.3 | 1510 | 0.584 | 23.5 | 460 | 0.269 | 984 | 6310 | 164 | ND | |
|
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| Average | 61.3 | 1800 | 38.7 | 1593 | 0.538 | 19.6 | 482 | 0.415 | 1010 | 6225 | 165 | 1.54 | |
| %RSD | 5.42 | 4.33 | 4.75 | 4.36 | 12.2 | 20.0 | 4.40 | 29.3 | 2.25 | 3.26 | 1.73 | 22.9 | |
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| 4 | Day 1 | 66.9 | 1840 | 33.6 | 1640 | 0.420 | 12.7 | 492 | 0.513 | 1363 | 6454 | 208 | 1.71 |
| Day 2 | 63.3 | 1800 | 33.7 | 1520 | 9.09 | 17.0 | 474 | 0.530 | 1330 | 6704 | 204 | 2.98 | |
| Day 3 | 66.1 | 1840 | 32.9 | 1680 | ND | 22.1 | 492 | 0.243 | 1376 | 6950 | 208 | 1.04 | |
|
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| Average | 65.4 | 1827 | 33.4 | 1613 | 4.76 | 17.3 | 486 | 0.429 | 1356 | 6703 | 207 | 1.91 | |
| %RSD | 2.32 | 1.03 | 1.06 | 4.21 | 129 | 22.1 | 1.77 | 30.7 | 1.42 | 3.02 | 0.842 | 51.7 | |
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| 5 | Day 1 | 58.7 | 1740 | 37.5 | 1600 | ND | 18.7 | 489 | 0.647 | 710 | 5662 | 194 | 1.65 |
| Day 2 | 57.0 | 1720 | 37.8 | 1520 | 0.911 | 19.0 | 478 | 0.436 | 706 | 6182 | 191 | 2.13 | |
| Day 3 | 56.4 | 1680 | 35.1 | 1570 | 0.584 | 17.8 | 467 | 0.269 | 700 | 6258 | 189 | 5.16 | |
|
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| Average | 57.4 | 1713 | 36.8 | 2460 | 0.748 | 18.5 | 478 | 0.451 | 705 | 6034 | 191 | 2.98 | |
| %RSD | 1.73 | 1.46 | 3.27 | 1.34 | 31.0 | 2.65 | 1.90 | 34.3 | 0.569 | 4.39 | 1.19 | 52.2 | |
|
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| 6 | Day 1 | 61.4 | 1690 | 37.1 | 1680 | 1.22 | 20.1 | 465 | 0.447 | 1136 | 6923 | 198 | 1.75 |
| Day 2 | 60.9 | 1610 | 37.7 | 1570 | 0.391 | 18.3 | 455 | 0.396 | 1117 | 7160 | 201 | 1.82 | |
| Day 3 | 61.0 | 1660 | 36.0 | 1720 | ND | 27.5 | 455 | 0.243 | 1144 | 7312 | 194 | 1.92 | |
|
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| Average | 61.1 | 1653 | 36.9 | 1657 | 0.806 | 22.0 | 458 | 0.362 | 1132 | 7132 | 198 | 1.79 | |
| %RSD | 0.348 | 1.99 | 1.90 | 3.83 | 72.7 | 18.0 | 1.04 | 24.0 | 0.989 | 2.24 | 1.35 | 4.86 | |
|
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| Pool | Day 1 | 64.1 | 1730 | 34.9 | 1690 | 0.660 | 17.4 | 477 | 0.540 | 1016 | 6355 | 195 | 2.17 |
| Day 2 | 59.6 | 1690 | 35.5 | 1500 | 0.705 | 16.0 | 466 | 0.410 | 992 | 6416 | 194 | 2.06 | |
| Day 3 | 64.7 | 1830 | 35.3 | 1750 | 3.74 | 23.0 | 492 | 1.22 | 1040 | 6136 | 179 | ND | |
|
| |||||||||||||
| Average | 62.8 | 1750 | 35.2 | 1647 | 1.70 | 18.8 | 478 | 0.722 | 1016 | 6302 | 189 | 2.12 | |
| %RSD | 3.62 | 3.36 | 0.73 | 6.47 | 84.8 | 16.0 | 2.20 | 49.0 | 1.93 | 1.91 | 3.88 | 3.41 | |
|
| |||||||||||||
| Average | 61.3 | 1779 | 35.0 | 1754 | 1.79 | 21.8 | 480 | 0.490 | 1032 | 6825 | 197 | 1.96 | |
| % Diff from pool | −2.40 | 1.68 | −0.725 | 6.51 | 5.05 | 15.9 | 0.397 | −32.1 | 1.58 | 8.29 | 4.49 | −7.52 | |
Values reported in units of μg/mL
Values were not found to be greater than the IDL (Table 3)