Table I.
Data Collection and Refinement Statistics
| Data collection | |
|---|---|
| Space group | P2(1) |
| PDB ID | 3WJM |
| Cell dimensions | |
| a, b, c (Å) | 92.06, 205.02, 119.71 |
| Β (°) | 103.0 |
| Wavelength (Å) | 1.075 |
| Resolution (Å)a | 50–2.8 (2.85–2.8) |
| Rsym (%) | 7.7 (49.7) |
| I/σ(I) | 25.3 (4.4) |
| Completeness (%)a | 96.6 (89.8) |
| Redundancy | 3.5 (3.2) |
| Search model | 3GWJ |
| Refinement | |
| Resolution range (Å) | 50–2.8 (2.88–2.80) |
| No. reflections | 97,193 |
| Rwork (Rfree) (%) | 17.4/23.9 (22.2/32.1) |
| No. atoms | |
| Protein | 34,060 |
| Glycoside | 421 |
| Water | 120 |
| B-factors (Å2) | |
| Protein | 53.175 |
| Glycoside | 76.301 |
| Water | 37.677 |
| R.m.s. deviations | |
| Bond lengths (Å) | 0.012 |
| Bond angles (°) | 1.627 |
| % Favored (disallowed) in Ramachandran plot | 90.1 (0) |
a
Values for the highest resolution shell are in parentheses.