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. 2014 Jul 11;9(7):e100380. doi: 10.1371/journal.pone.0100380

Table 3. 1H NMR and 13C NMR-chemical shifts of GSP-2 a , b .

Glycosyl residue H-1/C-1 H-2/C-2 H-3/C-3 H-4/C-4 H-5/C-5 H-6a,H-6b/C-6
β-D-Glcp-(1→ 4.72 3.22 3.43 3.44 3.40 3.62, 3.82
A 103.3 73.8 75.8 70.2 76.0 60.9
→3)-β-D- Glcp-(1→ 4.70 3.42 3.65 3.35 3.38 3.62, 3.82
B 103.3 73.8 84.4 70.0 76.3 60.9
→4)-β-D -Glcp-(1→ 4.42 3.22 3.36 3.58 3.60 3.61, 3.80
C 103.3 74.0 73.9 78.5 75.1 60.9
→6)-β-D-Glcp-(1→ 4.41 3.22 3.43 3.44 3.58 3.77, 4.12
D 103.3 73.8 76.0 68.8 75.8 69.2
→3,6)-β-D-Glcp-(1→ 4.45 3.48 3.65 3.43 3.58 3.77, 4.12
E 103.3 73.9 84.4 68.8 76.0 69.2
a

Measured in 500/125 MHz, δ in ppm.

b

Values of 13C chemical shift were record with reference to TMS as internal standard.