Table 1. Data collection and refinement statistics.
| hsRio1/ATP/Mg2+ | |
|---|---|
| Data collection | |
| Space group | P3221 |
| Cell dimensions | |
| a = b, c (Å) | 78.76, 110.57 |
| α = β, γ (°) | 90.00, 120.00 |
| Resolution (Å) | 43.0–2.7 (2.80–2.70)a |
| Rsym or Rmerge | 0.066 (0.215)1 |
| I/σI | 12.7 (3.40)1 |
| Completeness (%) | 100 (100)1 |
| Redundancy | 2.0 (2.0)1 |
| Refinement | |
| Resolution (Å) | 43.0–2.7 (2.80–2.70) |
| No. reflections | 11330 (1101) |
| Rwork / Rfree | 20.4/24.3 (31.1/35.7)1 |
| No. atoms | 1924 |
| Protein | 1889 |
| Ligand/ion | 28 |
| Water | 7 |
| B-factors (average; Å2) | 58.8 |
| rms deviations | |
| Bond lengths (Å) | 0.011 |
| Bond angles (°) | 1.35 |
aOne crystal was used for each data set. Values in parentheses are for highest-resolution shell.