| Bruker APEXII CCD diffractometer | 5279 independent reflections |
| Radiation source: fine-focus sealed tube | 4117 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.034 |
| φ and ω scans | θmax = 27.5°, θmin = 1.6° |
| Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −16→16 |
| Tmin = 0.927, Tmax = 0.971 | k = −23→22 |
| 39926 measured reflections | l = −13→13 |