| Bruker SMART APEX CCD diffractometer | 8701 independent reflections |
| Radiation source: fine-focus sealed tube | 5402 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.080 |
| Detector resolution: 8.3660 pixels mm-1 | θmax = 28.4°, θmin = 1.9° |
| φ and ω scans | h = −11→11 |
| Absorption correction: multi-scan (SADABS; Bruker, 2013) | k = −14→14 |
| Tmin = 0.65, Tmax = 0.98 | l = −26→26 |
| 31443 measured reflections |
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