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. 2014 Jun 21;70(Pt 7):o802. doi: 10.1107/S160053681401383X
Cl2—C15 1.745 (2) C14—C15 1.377 (3)
Cl1—C1 1.739 (3) C14—C13 1.383 (3)
O2—C19 1.316 (3) C14—H14 0.9300
O2—C20 1.466 (3) C10—H10A 0.9700
C12—C13 1.382 (3) C10—H10B 0.9700
C12—C17 1.383 (3) C15—C16 1.367 (3)
C12—C11 1.519 (3) C8—H8A 0.9700
C18—N1 1.442 (3) C8—H8B 0.9700
C18—C19 1.529 (3) C13—H13 0.9300
C18—C11 1.556 (3) C20—C21 1.441 (4)
C18—C7 1.584 (3) C20—H20A 0.9700
N1—C22 1.144 (3) C20—H20B 0.9700
C11—C10 1.523 (3) C16—H16 0.9300
C11—H11 0.9800 C3—C2 1.376 (4)
C4—C3 1.373 (3) C3—H3 0.9300
C4—C5 1.382 (3) C5—C6 1.388 (4)
C4—C7 1.513 (3) C5—H5 0.9300
O1—C19 1.191 (3) C1—C2 1.352 (4)
C7—C8 1.532 (3) C1—C6 1.365 (4)
C7—H7 0.9800 C6—H6 0.9300
C9—O3 1.205 (3) C2—H2 0.9300
C9—C10 1.500 (3) C21—H21A 0.9600
C9—C8 1.502 (3) C21—H21B 0.9600
C17—C16 1.378 (3) C21—H21C 0.9600
C17—H17 0.9300
C19—O2—C20 117.11 (18) H10A—C10—H10B 108.0
C13—C12—C17 118.1 (2) C16—C15—C14 120.7 (2)
C13—C12—C11 122.58 (19) C16—C15—Cl2 119.88 (19)
C17—C12—C11 119.21 (19) C14—C15—Cl2 119.39 (18)
N1—C18—C19 106.80 (16) C9—C8—C7 110.72 (19)
N1—C18—C11 109.33 (17) C9—C8—H8A 109.5
C19—C18—C11 109.64 (16) C7—C8—H8A 109.5
N1—C18—C7 107.07 (16) C9—C8—H8B 109.5
C19—C18—C7 113.03 (17) C7—C8—H8B 109.5
C11—C18—C7 110.82 (15) H8A—C8—H8B 108.1
C22—N1—C18 177.6 (2) C12—C13—C14 121.2 (2)
C12—C11—C10 114.26 (17) C12—C13—H13 119.4
C12—C11—C18 114.07 (16) C14—C13—H13 119.4
C10—C11—C18 109.69 (16) C21—C20—O2 109.8 (2)
C12—C11—H11 106.0 C21—C20—H20A 109.7
C10—C11—H11 106.0 O2—C20—H20A 109.7
C18—C11—H11 106.0 C21—C20—H20B 109.7
C3—C4—C5 116.7 (2) O2—C20—H20B 109.7
C3—C4—C7 122.3 (2) H20A—C20—H20B 108.2
C5—C4—C7 120.9 (2) C15—C16—C17 119.6 (2)
C4—C7—C8 114.22 (18) C15—C16—H16 120.2
C4—C7—C18 114.57 (17) C17—C16—H16 120.2
C8—C7—C18 111.65 (16) C4—C3—C2 122.4 (3)
C4—C7—H7 105.1 C4—C3—H3 118.8
C8—C7—H7 105.1 C2—C3—H3 118.8
C18—C7—H7 105.1 C4—C5—C6 121.4 (3)
O1—C19—O2 126.2 (2) C4—C5—H5 119.3
O1—C19—C18 124.5 (2) C6—C5—H5 119.3
O2—C19—C18 109.36 (17) C2—C1—C6 120.4 (3)
O3—C9—C10 122.4 (2) C2—C1—Cl1 119.6 (2)
O3—C9—C8 122.6 (2) C6—C1—Cl1 120.0 (2)
C10—C9—C8 114.99 (18) C1—C6—C5 119.5 (3)
C16—C17—C12 121.2 (2) C1—C6—H6 120.2
C16—C17—H17 119.4 C5—C6—H6 120.2
C12—C17—H17 119.4 C1—C2—C3 119.6 (3)
C15—C14—C13 119.1 (2) C1—C2—H2 120.2
C15—C14—H14 120.4 C3—C2—H2 120.2
C13—C14—H14 120.4 C20—C21—H21A 109.5
C9—C10—C11 111.22 (18) C20—C21—H21B 109.5
C9—C10—H10A 109.4 H21A—C21—H21B 109.5
C11—C10—H10A 109.4 C20—C21—H21C 109.5
C9—C10—H10B 109.4 H21A—C21—H21C 109.5
C11—C10—H10B 109.4 H21B—C21—H21C 109.5
C19—C18—N1—C22 −164 (6) C7—C18—C19—O2 59.8 (2)
C11—C18—N1—C22 78 (6) C13—C12—C17—C16 −1.5 (3)
C7—C18—N1—C22 −43 (6) C11—C12—C17—C16 175.7 (2)
C13—C12—C11—C10 41.3 (3) O3—C9—C10—C11 −160.1 (2)
C17—C12—C11—C10 −135.7 (2) C8—C9—C10—C11 20.6 (3)
C13—C12—C11—C18 −86.0 (2) C12—C11—C10—C9 166.34 (18)
C17—C12—C11—C18 96.9 (2) C18—C11—C10—C9 −64.1 (2)
N1—C18—C11—C12 55.2 (2) C13—C14—C15—C16 −2.0 (4)
C19—C18—C11—C12 −61.5 (2) C13—C14—C15—Cl2 177.18 (17)
C7—C18—C11—C12 173.01 (17) O3—C9—C8—C7 −139.3 (2)
N1—C18—C11—C10 −74.4 (2) C10—C9—C8—C7 40.1 (3)
C19—C18—C11—C10 168.84 (17) C4—C7—C8—C9 169.06 (18)
C7—C18—C11—C10 43.4 (2) C18—C7—C8—C9 −58.9 (2)
C3—C4—C7—C8 11.8 (3) C17—C12—C13—C14 1.1 (3)
C5—C4—C7—C8 −164.7 (2) C11—C12—C13—C14 −176.0 (2)
C3—C4—C7—C18 −118.7 (2) C15—C14—C13—C12 0.7 (3)
C5—C4—C7—C18 64.7 (3) C19—O2—C20—C21 140.9 (3)
N1—C18—C7—C4 −93.2 (2) C14—C15—C16—C17 1.6 (4)
C19—C18—C7—C4 24.1 (2) Cl2—C15—C16—C17 −177.61 (19)
C11—C18—C7—C4 147.63 (18) C12—C17—C16—C15 0.2 (4)
N1—C18—C7—C8 134.96 (19) C5—C4—C3—C2 1.1 (4)
C19—C18—C7—C8 −107.7 (2) C7—C4—C3—C2 −175.6 (2)
C11—C18—C7—C8 15.8 (2) C3—C4—C5—C6 −0.8 (4)
C20—O2—C19—O1 −0.1 (3) C7—C4—C5—C6 176.0 (2)
C20—O2—C19—C18 179.17 (17) C2—C1—C6—C5 1.3 (4)
N1—C18—C19—O1 −3.5 (3) Cl1—C1—C6—C5 −177.6 (2)
C11—C18—C19—O1 114.8 (2) C4—C5—C6—C1 −0.4 (4)
C7—C18—C19—O1 −121.0 (2) C6—C1—C2—C3 −1.0 (4)
N1—C18—C19—O2 177.26 (16) Cl1—C1—C2—C3 178.0 (2)
C11—C18—C19—O2 −64.4 (2) C4—C3—C2—C1 −0.2 (4)