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. 2014 Jun 25;70(Pt 7):o809–o810. doi: 10.1107/S1600536814014317
O1—C10 1.2192 (18) C19—C20 1.369 (2)
C1—C2 1.499 (2) C20—C21 1.375 (3)
C2—C3 1.3873 (18) C21—C22 1.385 (2)
C2—C7 1.4072 (16) C1—H1A 0.9600
C3—C4 1.370 (2) C1—H1B 0.9600
C4—C5 1.376 (2) C1—H1C 0.9600
C5—C6 1.377 (2) C3—H3 0.9300
C6—C7 1.388 (2) C4—H4 0.9300
C7—C8 1.4628 (17) C5—H5 0.9300
C8—C9 1.3207 (17) C6—H6 0.9300
C9—C10 1.4743 (19) C8—H8 0.9300
C10—C11 1.4917 (16) C9—H9 0.9300
C11—C12 1.3901 (19) C12—H12 0.9300
C11—C16 1.3904 (18) C13—H13 0.9300
C12—C13 1.3828 (17) C15—H15 0.9300
C13—C14 1.3909 (18) C16—H16 0.9300
C14—C15 1.3948 (18) C18—H18 0.9300
C14—C17 1.4847 (16) C19—H19 0.9300
C15—C16 1.3809 (16) C20—H20 0.9300
C17—C18 1.3900 (19) C21—H21 0.9300
C17—C22 1.384 (2) C22—H22 0.9300
C18—C19 1.3840 (18)
C1—C2—C3 120.06 (11) C2—C1—H1C 109.00
C1—C2—C7 121.73 (11) H1A—C1—H1B 109.00
C3—C2—C7 118.16 (12) H1A—C1—H1C 109.00
C2—C3—C4 122.16 (12) H1B—C1—H1C 109.00
C3—C4—C5 119.78 (14) C2—C3—H3 119.00
C4—C5—C6 119.30 (15) C4—C3—H3 119.00
C5—C6—C7 121.79 (13) C3—C4—H4 120.00
C2—C7—C6 118.80 (12) C5—C4—H4 120.00
C2—C7—C8 120.48 (12) C4—C5—H5 120.00
C6—C7—C8 120.72 (11) C6—C5—H5 120.00
C7—C8—C9 126.52 (13) C5—C6—H6 119.00
C8—C9—C10 122.06 (13) C7—C6—H6 119.00
O1—C10—C9 121.45 (11) C7—C8—H8 117.00
O1—C10—C11 119.84 (12) C9—C8—H8 117.00
C9—C10—C11 118.70 (12) C8—C9—H9 119.00
C10—C11—C12 122.41 (11) C10—C9—H9 119.00
C10—C11—C16 118.91 (11) C11—C12—H12 120.00
C12—C11—C16 118.59 (11) C13—C12—H12 120.00
C11—C12—C13 120.66 (12) C12—C13—H13 119.00
C12—C13—C14 121.08 (13) C14—C13—H13 119.00
C13—C14—C15 117.89 (11) C14—C15—H15 119.00
C13—C14—C17 120.99 (12) C16—C15—H15 119.00
C15—C14—C17 121.12 (11) C11—C16—H16 120.00
C14—C15—C16 121.17 (12) C15—C16—H16 120.00
C11—C16—C15 120.55 (12) C17—C18—H18 120.00
C14—C17—C18 120.50 (12) C19—C18—H18 120.00
C14—C17—C22 121.33 (12) C18—C19—H19 120.00
C18—C17—C22 118.16 (11) C20—C19—H19 120.00
C17—C18—C19 120.97 (14) C19—C20—H20 120.00
C18—C19—C20 120.12 (14) C21—C20—H20 120.00
C19—C20—C21 119.72 (13) C20—C21—H21 120.00
C20—C21—C22 120.46 (17) C22—C21—H21 120.00
C17—C22—C21 120.57 (15) C17—C22—H22 120.00
C2—C1—H1A 109.00 C21—C22—H22 120.00
C2—C1—H1B 109.00
C1—C2—C3—C4 −178.74 (14) C16—C11—C12—C13 −1.5 (2)
C7—C2—C3—C4 −1.1 (2) C10—C11—C16—C15 −176.84 (13)
C1—C2—C7—C6 177.97 (13) C12—C11—C16—C15 −0.2 (2)
C1—C2—C7—C8 −2.3 (2) C11—C12—C13—C14 1.5 (2)
C3—C2—C7—C6 0.4 (2) C12—C13—C14—C15 0.3 (2)
C3—C2—C7—C8 −179.93 (14) C12—C13—C14—C17 −179.94 (14)
C2—C3—C4—C5 1.1 (2) C13—C14—C15—C16 −2.0 (2)
C3—C4—C5—C6 −0.3 (2) C17—C14—C15—C16 178.22 (13)
C4—C5—C6—C7 −0.4 (2) C13—C14—C17—C18 40.6 (2)
C5—C6—C7—C2 0.4 (2) C13—C14—C17—C22 −140.18 (15)
C5—C6—C7—C8 −179.34 (14) C15—C14—C17—C18 −139.63 (15)
C2—C7—C8—C9 161.41 (14) C15—C14—C17—C22 39.6 (2)
C6—C7—C8—C9 −18.9 (2) C14—C15—C16—C11 2.0 (2)
C7—C8—C9—C10 178.77 (13) C14—C17—C18—C19 179.54 (14)
C8—C9—C10—O1 13.9 (2) C22—C17—C18—C19 0.3 (2)
C8—C9—C10—C11 −164.91 (13) C14—C17—C22—C21 −179.96 (16)
O1—C10—C11—C12 −158.73 (15) C18—C17—C22—C21 −0.7 (2)
O1—C10—C11—C16 17.8 (2) C17—C18—C19—C20 −0.1 (2)
C9—C10—C11—C12 20.1 (2) C18—C19—C20—C21 0.4 (3)
C9—C10—C11—C16 −163.39 (13) C19—C20—C21—C22 −0.8 (3)
C10—C11—C12—C13 175.01 (14) C20—C21—C22—C17 1.0 (3)