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. 2014 Jun 25;70(Pt 7):o809–o810. doi: 10.1107/S1600536814014317
Bruker Kappa APEXII CCD diffractometer 4534 independent reflections
Radiation source: fine-focus sealed tube 3291 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.024
ω and φ scan θmax = 29.6°, θmin = 2.2°
Absorption correction: multi-scan (SADABS; Bruker, 2004) h = −10→10
Tmin = 0.908, Tmax = 1.000 k = −13→13
18636 measured reflections l = −16→16