| Bruker Kappa APEXII CCD diffractometer | 4534 independent reflections |
| Radiation source: fine-focus sealed tube | 3291 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.024 |
| ω and φ scan | θmax = 29.6°, θmin = 2.2° |
| Absorption correction: multi-scan (SADABS; Bruker, 2004) | h = −10→10 |
| Tmin = 0.908, Tmax = 1.000 | k = −13→13 |
| 18636 measured reflections | l = −16→16 |