| Stoe IPDS 1 diffractometer | 1548 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.035 |
| Plane graphite monochromator | θmax = 25.9°, θmin = 2.0° |
| φ rotation scans | h = −5→5 |
| 7822 measured reflections | k = −25→25 |
| 1958 independent reflections | l = −14→14 |