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. 2014 Jun 23;70(Pt 7):18–22. doi: 10.1107/S1600536814009519
Stoe IPDS 1 diffractometer 1548 reflections with I > 2σ(I)
Radiation source: fine-focus sealed tube Rint = 0.035
Plane graphite monochromator θmax = 25.9°, θmin = 2.0°
φ rotation scans h = −5→5
7822 measured reflections k = −25→25
1958 independent reflections l = −14→14