| Bruker Kappa APEXII diffractometer | 5962 independent reflections |
| Radiation source: fine-focus sealed tube | 4098 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.035 |
| Detector resolution: 0 pixels mm-1 | θmax = 27.0°, θmin = 1.9° |
| ω and φ scans | h = −19→11 |
| Absorption correction: multi-scan (SADABS; Bruker, 2004) | k = −18→18 |
| Tmin = 0.967, Tmax = 0.974 | l = −15→15 |
| 30073 measured reflections |