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. 2014 Jun 25;70(Pt 7):o816–o817. doi: 10.1107/S1600536814014391
Bruker Kappa APEXII diffractometer 5962 independent reflections
Radiation source: fine-focus sealed tube 4098 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.035
Detector resolution: 0 pixels mm-1 θmax = 27.0°, θmin = 1.9°
ω and φ scans h = −19→11
Absorption correction: multi-scan (SADABS; Bruker, 2004) k = −18→18
Tmin = 0.967, Tmax = 0.974 l = −15→15
30073 measured reflections