| Siemens SMART CCD diffractometer | 3196 independent reflections |
| Radiation source: fine-focus sealed tube | 2587 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.000 |
| ω scans | θmax = 30.6°, θmin = 2.3° |
| Absorption correction: multi-scan (TWINABS; Bruker, 2008) | h = −12→12 |
| Tmin = 0.253, Tmax = 0.746 | k = 0→13 |
| 3196 measured reflections | l = 0→18 |
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