Table 3. Experimental details.
| Crystal data | |
| Chemical formula | Pb3[IO4(OH)2]2 |
| M r | 1071.40 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 296 |
| a, b, c (Å) | 8.9653 (9), 9.2113 (9), 12.8052 (13) |
| β (°) | 101.042 (2) |
| V (Å3) | 1037.90 (18) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 54.55 |
| Crystal size (mm) | 0.06 × 0.06 × 0.05 |
| Data collection | |
| Diffractometer | Siemens SMART CCD |
| Absorption correction | Multi-scan (TWINABS; Bruker, 2008 ▶) |
| T min, T max | 0.253, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 3196, 3196, 2587 |
| (sin θ/λ)max (Å−1) | 0.716 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.041, 0.087, 1.07 |
| No. of reflections | 3196 |
| No. of parameters | 94 |
| H-atom treatment | H-atom parameters not refined |
| Δρmax, Δρmin (e Å−3) | 2.88, −1.95 |