Bruker SMART BREEZE CCD diffractometer | 2983 reflections with I > 2σ(I) |
Radiation source: 2 kW sealed X-ray tube | Rint = 0.072 |
φ and ω scans | θmax = 27.6°, θmin = 2.0° |
Absorption correction: multi-scan (SADABS; Bruker, 2012) | h = −9→9 |
Tmin = 0.919, Tmax = 1.000 | k = −13→13 |
19956 measured reflections | l = −17→18 |
4752 independent reflections |