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. Author manuscript; available in PMC: 2015 Feb 1.
Published in final edited form as: J Liq Chromatogr Relat Technol. 2013 Dec 11;37(4):572–587. doi: 10.1080/10826076.2012.749499

Table 1.

The K-values of main components in Jiubiying extracts in two-phase solvent systems.

Solvent system (v/v) K
Syringin (II) Syringaresinol 4′,4″-O-β-D-bis- glucopyranoside (I) Syringaresinol 4′-O-β-D-glucopyranoside (IV) Pedunculoside (V)
n-Heptane-n-butanol-acetonitrile-water (2:3.8:1.2:4) 0.15 0.01 0.75 15.32
n-Heptane-n-butanol-acetonitrile-water (1:4.4:0.6:4) 0.33 0.01 2.71 71.53
n-Butanol-water (1:1) 0.76 0.13 10.24 165.0
Ethyl acetate-n-butanol-water (4:1:5) 0.12 0.06 0.63 196.3
Ethyl acetate-n-butanol-water (3:2:5) 0.33 0.01 7.88 220.2
Ethyl acetate-n-butanol-water (1:4:5) 0.54 0.10 6.69 66.50
Ethyl acetate-n-butanol-water (1:6:7) 0.66 0.09 10.35 96.48