Skip to main content
. 2014 Jul 10;136(30):10573–10576. doi: 10.1021/ja505371z

Figure 2.

Figure 2

(a) 1H NMR spectra of the conversion of 18 mM TrtSSH (blue circle) to TrtSH (red circle) with 1 equiv of [NBu4+][TFA–] recorded every 60 s. (b) Addition of PPh3 (yellow circle) in 0.5 equiv. increments at the end of the reaction shows the clean formation of Ph3PS (green circle).