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. Author manuscript; available in PMC: 2015 Aug 1.
Published in final edited form as: Bioorg Med Chem. 2014 May 23;22(15):4257–4268. doi: 10.1016/j.bmc.2014.05.036

Table 1.

Products from oxidation reactions

Entry Reactant Condition Product HRMS
1 25 TEMPO (0.7 eq), BAIB (4 eq), CH3CN-H2O, rt, 16h graphic file with name nihms601182t1.jpg [M+H]+: 519.3119
2 24 RuCl3 (0.7 eq), NaIO4 (4 eq), CH3CN-CCl4-H2O, rt, 7h graphic file with name nihms601182t2.jpg [M+H]+: 350.1656
[M+H3O]+: 368.1762
3 20 (+21) RuCl3 (0.7 eq), NaIO4 (4 eq), CH3CN-CCl4-H2O, 50 °C, 2days graphic file with name nihms601182t3.jpg [M+H]+: 494.2609
[M+H3O]+: 512.2742