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. Author manuscript; available in PMC: 2014 Aug 11.
Published in final edited form as: J Nat Prod. 2014 Feb 5;77(2):304–310. doi: 10.1021/np400899a

Table 2.

1H Spin Systems and Sequential Assignments of ASPE Using DQF-COSY, TOCSY, NOESY, and HSQC Spectra (in CD3OH, 900 MHz)

1H spin systems amino acids residue no.
AX Gly 3, 5, 24, 28
AMX Asp, Asn, Cys, Ser 1, 8, 9, 13, 15, 16, 21, 25, 30
A3B3MX Val 10
A3MX Thr 20
A3B3MPTX Leu 19
A3MPT(B3)X Ile 22, 29, 32, 33
AM(PT)X Glu, Gln 4, 6, 7, 11
A2(T2)MPX Pro 2, 14, 17, 18, 23, 26
AMX + AMM′XX′ Phe 12
AMX +AA′XX′ Tyr 27, 31