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. 2014 Aug 4;16(16):4308–4311. doi: 10.1021/ol502023d

Scheme 3. Allylation of Nitroalkanes via CO2 Activation,b.

Scheme 3

Nitroalkane (0.3 mmol) and allyl alcohol (0.45 mmol) in 1.75 mL of DMSO under 1 atm of CO2. b Isolated yields. c Ar replaced CO2 (% conversion via crude 1H NMR). d Allyl alcohol (0.9 mmol), 160 °C, 20 min in a microwave reactor.