TABLE 2.
Two-Shell Simulations of Fourier Peaks I and IIa
sampleb | Mn–O interaction
|
σ 21c | Mn–Mn interaction
|
σ 22c | ΔE0 | Φ × 103 d | ε2 × 105 d | ||
---|---|---|---|---|---|---|---|---|---|
R1(Å) | N1 | R2(Å) | N2 | ||||||
CDS1A | 1.85 | 3.67 | 0.0096 | 2.71 | 1.04 | 0.0040 | −17 | 0.81 | 1.57 |
CDS1B | 1.85 | 4.34 | 0.0101 | 2.72 | 0.91 | 0.0020 | −18 | 0.68 | 1.35 |
CDS2 | 1.82 | 2.30 | 0.0060 | 2.70 | 1.09 | 0.0020 | −21 | 0.60 | 1.16 |
CDS3A | 1.83 | 3.71 | 0.0100 | 2.71 | 0.92 | 0.0016 | −21 | 0.41 | 0.79 |
CDS3B | 1.83 | 2.49 | 0.0080 | 2.71 | 0.91 | 0.0030 | −20 | 0.70 | 1.38 |
CDS3C | 1.87 | 2.57 | 0.0080 | 2.75 | 0.89 | 0.0030 | −12 | 0.85 | 1.69 |
Fit parameters are as defined in the text. S02 = 0.85 in all fits. Data were fit k = 3.7–11.2 Å−1. The width of the Fourier isolation window employed was 2 Å.
CDS1A and CDS1B are S1′-state samples; CDS2 is an S2′-state sample; CDS3A, B, C are S3′-state samples.
Units are Å2.
Goodness-of-fit parameters Φ and ε2 are defined in refs 35 and 36. Φ is the fit error function normalized to the amplitude of the EXAFS oscillations. ε2 is Φ with the number of floating parameters taken into account. N1 and N2 correspond to the average number of O and Mn scatterers at distances R1 and R2 around an absorbing Mn atom.