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. 2013 May 6;52(25):6464–6467. doi: 10.1002/anie.201302634

Scheme 2.

Scheme 2

Synthesis of molecular Solomon link 6. Reaction conditions: a) FeCl2, 2,2′-(ethylenedioxy)bis(ethylamine), DMSO, 60 °C, 24 h; b) excess KPF6 (aq), 75 % (over two steps).