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. 2014 May 9;289(26):18110–18120. doi: 10.1074/jbc.M114.555862

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© 2014 by The American Society for Biochemistry and Molecular Biology, Inc.

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FIGURE 5. — Structural determination for UDP-QuiNAc. A, structure and proton NMR resonance assignments of the reaction product deduced to be UDP-d-QuiNAc. B–D, two-dimensional ¹H-¹H TOCSY, COSY, and NOESY analysis of UDP-QuiNAc. B, two-dimensional ¹H-¹H TOCSY correlation map for UDP-QuiNAc. C, two-dimensional ¹H-¹H COSY correlation map for UDP-QuiNAc. The experiment was acquired in real time mode; therefore, all resonances with chemical shifts beyond water appear mirrored. D, two-dimensional ¹H-¹H NOESY correlation map for UDP-QuiNAc.