Table 1.
Glycans | Relative abundance |
||||||
---|---|---|---|---|---|---|---|
NMRa) | CGEb) | LC-MSc) | MALDI-MS | MALDI-MS permethylated |
LC-ESI-MS MS permethylated |
LC-MALDI permethylated |
|
Man 5 | 57 | 51.5 | 52 ± 2 | 51 ± 1 | 59.0 ± 0.6 | 53.5 ± 0.4 | 50 ± 6 |
Man 6 | 31 | 30.3 | 32 ± 2 | 27.4 ± 0.7 | 29.0 ± 0.7 | 32.5 ± 0.6 | 30 ± 5 |
Man 7 | 4 | 4 | 6.3 ± 0.6 | 7 ± 1 | 4.0 ± 0.2 | 8.0 ± 0.2 | 11 ± 4 |
Man 8 | 7 | 8.5 | 7.2 ± 0.8 | 10.9 ± 0.6 | 7.0 ± 0.2 | 5.2 ± 0.3 | 8 ± 4 |
Man 9 | 1 | 3.7 | 1.6 ± 0.1 | 3.5 ± 0.6 | 1.00 ± 0.05 | 0.82 ± 0.06 | 2 ± 1 |