Table 1.
Data collection and refinement statistics.
| Space Group | C2 |
|---|---|
| Unit cell dimensions | 226.4, 133.9, 93.5, 90, 91.4, 90 |
| Resolution range (Å) | 43.5-2.83 (2.90-2.83)a |
| Unique reflections | 124259 (8574) |
| Average redundancy | 2.0 |
| Completeness (%) | 94.3 (87.7) |
| Rsym | 6.1% (51.5%) |
| <I/sigI> | 12.6 (2.0) |
| Rwork/Rfree | 24.8/28.0 (33.3/33.8) |
| Rms bond length (Å) | 0.008 |
| Rms bond angle (Deg) | 0.978 |
| Ramachandran outliersb | 5 (0.26%) |
| Ramachandran favored | 1897 (97.6%) |
| Number of residues per AU | 2238 (three fullE•cyto-GspL complexes) |
| Number of water molecules | 16 |
| Average B factors (Å2): | |
| Protein | 59.4 |
| AMPPNP | 38.1 |
| Zn | 56.3 |
a
Values in parenthesis correspond to the highest-resolution shell.
b
Calculated using the Molprobity server (Chen et al., 2010).