Table 4. Recovery analysis of the STG spiked in cereal and oil products.
Matrix | Expected(ng/g) | IAC-icELISA Founda (ng/g) | Recovery (%) | HPLC-MS/MS Founda (ng/g) | Recovery (%) | |
Wheat | Within assayb (n = 6) | 5 | 5.40±0.40 | 108.0 | 4.51±0.21 | 90.2 |
10 | 9.62±0.45 | 96.2 | 9.67±0.35 | 96.7 | ||
20 | 18.90±0.78 | 94.5 | 20.06±0.64 | 100.3 | ||
Between assayc (n = 6) | 5 | 5.51±0.53 | 110.2 | 4.57±0.08 | 91.4 | |
10 | 9.46±0.61 | 94.6 | 9.56±0.04 | 95.6 | ||
20 | 19.40±0.97 | 97.0 | 20.64±0.13 | 103.2 | ||
Maize | Within assayb (n = 6) | 5 | 4.61±0.37 | 92.2 | 4.59±0.18 | 91.8 |
10 | 10.2±0.51 | 102.8 | 9.69±0.27 | 96.9 | ||
20 | 20.06±0.74 | 100.3 | 20.48±0.34 | 102.4 | ||
Between assayc (n = 6) | 5 | 4.53±0.41 | 90.6 | 4.63±0.11 | 92.6 | |
10 | 9.71±0.89 | 97.1 | 9.87±0.08 | 98.7 | ||
20 | 19.85±1.04 | 99.3 | 20.88±0.20 | 104.4 | ||
Peanut | Within assayb (n = 6) | 5 | 4.17±0.18 | 83.4 | 4.55±0.13 | 91.0 |
10 | 8.74±0.51 | 87.4 | 9.33±0.25 | 93.3 | ||
20 | 18.65±1.21 | 93.3 | 18.92±0.17 | 94.6 | ||
Between assayc (n = 6) | 5 | 4.39±0.30 | 87.8 | 4.52±0.09 | 90.4 | |
10 | 9.21±0.75 | 92.1 | 9.25±0.14 | 92.5 | ||
20 | 20.14±1.67 | 100.7 | 18.88±0.08 | 94.4 |
The reported data are the mean ± SD.
The assays are carried out in six replicates on the same day.
The assays are carried out in six different days.