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. 2014 Sep 3;9(9):e106415. doi: 10.1371/journal.pone.0106415

Table 4. Recovery analysis of the STG spiked in cereal and oil products.

Matrix Expected(ng/g) IAC-icELISA Founda (ng/g) Recovery (%) HPLC-MS/MS Founda (ng/g) Recovery (%)
Wheat Within assayb (n = 6) 5 5.40±0.40 108.0 4.51±0.21 90.2
10 9.62±0.45 96.2 9.67±0.35 96.7
20 18.90±0.78 94.5 20.06±0.64 100.3
Between assayc (n = 6) 5 5.51±0.53 110.2 4.57±0.08 91.4
10 9.46±0.61 94.6 9.56±0.04 95.6
20 19.40±0.97 97.0 20.64±0.13 103.2
Maize Within assayb (n = 6) 5 4.61±0.37 92.2 4.59±0.18 91.8
10 10.2±0.51 102.8 9.69±0.27 96.9
20 20.06±0.74 100.3 20.48±0.34 102.4
Between assayc (n = 6) 5 4.53±0.41 90.6 4.63±0.11 92.6
10 9.71±0.89 97.1 9.87±0.08 98.7
20 19.85±1.04 99.3 20.88±0.20 104.4
Peanut Within assayb (n = 6) 5 4.17±0.18 83.4 4.55±0.13 91.0
10 8.74±0.51 87.4 9.33±0.25 93.3
20 18.65±1.21 93.3 18.92±0.17 94.6
Between assayc (n = 6) 5 4.39±0.30 87.8 4.52±0.09 90.4
10 9.21±0.75 92.1 9.25±0.14 92.5
20 20.14±1.67 100.7 18.88±0.08 94.4
a

The reported data are the mean ± SD.

b

The assays are carried out in six replicates on the same day.

c

The assays are carried out in six different days.