Table 3. Data collection and processing.
Values in parentheses are for the outer shell.
| Diffraction source | Synchrotron |
| Wavelength (Å) | 0.972400 |
| Temperature (°C) | −173 |
| Detector | ADSC |
| Crystal-to-detector distance (mm) | 458.842 |
| Rotation range per image (°) | 2.0 |
| Total rotation range (°) | 182 |
| Exposure time per image (s) | 0.9 |
| Space group | P41212 |
| a, b, c (Å) | 115.351, 115.351, 123.663 |
| α, β, γ (°) | 90.000, 90.000, 90.000 |
| Mosaicity (°) | 0.185 |
| Resolution range (Å) | 49.27–3.71 |
| Total No. of reflections | 130664 |
| No. of unique reflections | 9350 |
| Completeness (%) | 99.7 (99.4) |
| 〈I/σ(I)〉 | 27.56 (10.57) |
| R meas (%) | 6.4 (27.6) |
| Overall B factor from Wilson plot (Å2) | 90.178 |
| Twinning analysis | |
| Statistics independent of twin laws | |
| 〈I 2〉/〈I〉2 | 2.204 |
| 〈F〉2/〈F 2〉 | 0.775 |
| 〈|E 2 − 1|〉 | 0.759 |
| 〈|L|〉, 〈L 2〉 | 0.476, 0.307 |
| Multivariate Z-score L-test | 1.082 |