Table 1. Data collection and processing.
Values in parentheses are for the outer shell.
| Diffraction source | EMBL P13, PETRA III storage ring |
| Wavelength (Å) | 1.033 |
| Temperature (K) | 100 |
| Detector | Dectris PILATUS 6M |
| Crystal-to-detector distance (mm) | 506.52 |
| Rotation range per image (°) | 0.05 |
| Total rotation range (°) | 90 |
| Exposure time per image (s) | 0.1 |
| Space group | P62 |
| a, b, c (Å) | 80.67, 80.67, 169.18 |
| α, β, γ (°) | 90, 90, 120 |
| Mosaicity (°) | 0.16 |
| Resolution range (Å) | 66.66–2.46 (2.56–2.46) |
| Total No. of reflections | 107891 (7226) |
| No. of unique reflections | 12434 (1284) |
| Completeness (%) | 99.4 (94.9) |
| Multiplicity | 8.7 (5.6) |
| 〈I/σ(I)〉 | 12.1 (3.4) |
| R r.i.m † | 0.105 (0.472) |
| Overall B factor from Wilson plot (Å2) | 57.06 |
†
Estimated by multiplying the conventional R merge value by the factor [N/(N − 1)]1/2, where N is the data multiplicity [R merge = 0.099 (0.428), data multiplicity = 8.7 (5.6)].