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. 2014 Aug 27;70(Pt 9):1260–1263. doi: 10.1107/S2053230X14017397

Table 3. Data collection and processing.

Values in parentheses are for the outer shell.

Diffraction source Beamline 5C, PAL
Wavelength (Å) 0.9795
Temperature (K) 100
Detector ADSC Q315r
Crystal-to-detector distance (mm) 150
Rotation range per image (°) 1
Total rotation range (°) 360
Exposure time per image (s) 1
Space group P61
a, b, c (Å) 78.4, 78.4, 49.5
α, β, γ (°) 90, 90, 120
Mosaicity (°) 0.263
Resolution range (Å) 30.00–1.50 (1.53–1.50)
Total No. of reflections 307105
No. of unique reflections 27818
Completeness (%) 99.76 (99.89)
Multiplicity 11.0 (8.5)
I/σ(I)〉 59 (6.63)
R r.i.m. (%) 6.92 (36.09)
Overall B factor from Wilson plot (Å2) 14.8