Table 1. Data collection and processing.
Diffraction source | MX beamline I04-1, DLS |
Wavelength (Å) | 0.9173 |
Temperature (K) | 100 |
Detector | PILATUS 2M |
Crystal-to-detector distance (mm) | 300.9 |
Rotation range per image (°) | 0.5 |
Total rotation range (°) | 180 |
Exposure time per image (s) | 0.5 |
Space group | C2 |
a, b, c (Å) | 213.53, 83.72, 66.95 |
α, β, γ (°) | 90, 102.53, 90 |
Mosaicity (°) | 0.278 |
Resolution range (Å) | 48.13–2.763 (2.862–2.763) |
Total No. of reflections | 112311 (10224) |
No. of unique reflections | 28294 (2621) |
Completeness (%) | 95.22 (88.86) |
Multiplicity | 4.0 (3.9) |
〈I/σ(I)〉 | 8.98 (2.11) |
R r.i.m. | 0.183 |
Overall B factor from Wilson plot (Å2) | 45.01 |