| Bruker Kappa APEXII diffractometer | 3475 independent reflections |
| Radiation source: fine-focus sealed tube | 2812 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.027 |
| Detector resolution: 0 pixels mm-1 | θmax = 27.0°, θmin = 2.2° |
| ω and φ scans | h = −12→12 |
| Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | k = −17→17 |
| Tmin = 0.977, Tmax = 0.981 | l = −15→15 |
| 37690 measured reflections |