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. 2014 Jul 23;70(Pt 8):o872. doi: 10.1107/S1600536814016365
Bruker Kappa APEXII diffractometer 3475 independent reflections
Radiation source: fine-focus sealed tube 2812 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.027
Detector resolution: 0 pixels mm-1 θmax = 27.0°, θmin = 2.2°
ω and φ scans h = −12→12
Absorption correction: multi-scan (SADABS; Sheldrick, 1996) k = −17→17
Tmin = 0.977, Tmax = 0.981 l = −15→15
37690 measured reflections