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. 2014 Jul 19;70(Pt 8):77–79. doi: 10.1107/S1600536814014251

Table 1. Experimental details.

Crystal data
Chemical formula C14H22N2O2Si2
M r 306.5
Crystal system, space group Monoclinic, P21/n
Temperature (K) 100
a, b, c (Å) 8.0770 (5), 11.2234 (6), 9.4377 (6)
β (°) 97.7087 (19)
V3) 847.81 (9)
Z 2
Radiation type Mo Kα
μ (mm−1) 0.21
Crystal size (mm) 0.65 × 0.26 × 0.12
 
Data collection
Diffractometer Bruker Kappa APEXII CCD
Absorption correction Multi-scan (SADABS; Bruker, 2013)
T min, T max 0.94, 0.98
No. of measured, independent and observed [I > 3σ(I)] reflections 15160, 2487, 2123
R int 0.024
(sin θ/λ)max−1) 0.705
 
Refinement
R[F 2 > 3σ(F 2)], wR(F 2), S 0.030, 0.042, 2.38
No. of reflections 2487
No. of parameters 91
H-atom treatment H-atom parameters constrained
Δρmax, Δρmin (e Å−3) 0.38, −0.20

Computer programs: APEX2 and SAINT-Plus (Bruker, 2013), SUPERFLIP (Palatinus & Chapuis, 2007), JANA2006 (Petříček, et al., 2014), Mercury (Macrae et al., 2008) and publCIF (Westrip, 2010).