Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C17H15ClN2O2 |
| M r | 314.76 |
| Crystal system, space group | Triclinic, P
|
| Temperature (K) | 100 |
| a, b, c (Å) | 5.6966 (6), 10.6852 (13), 12.7750 (17) |
| α, β, γ (°) | 101.573 (7), 100.620 (7), 101.311 (6) |
| V (Å3) | 726.47 (15) |
| Z | 2 |
| Radiation type | Cu Kα |
| μ (mm−1) | 2.40 |
| Crystal size (mm) | 0.55 × 0.1 × 0.05 |
| Data collection | |
| Diffractometer | Bruker SMART 6000 |
| Absorption correction | Multi-scan (SADABS; Bruker, 2003 ▶) |
| T min, T max | 0.695, 0.887 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 13302, 2723, 2053 |
| R int | 0.093 |
| (sin θ/λ)max (Å−1) | 0.614 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.064, 0.171, 1.06 |
| No. of reflections | 2723 |
| No. of parameters | 212 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.49, −0.52 |