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. 2014 Jul 19;70(Pt 8):80–83. doi: 10.1107/S1600536814014779
U11 U22 U33 U12 U13 U23
Cd1 0.0242 (5) 0.0207 (5) 0.0097 (4) −0.0101 (4) −0.0019 (4) 0.0028 (4)
Cd2 0.0155 (5) 0.0196 (5) 0.0088 (4) −0.0055 (4) 0.0000 (3) 0.0000 (3)
O1 0.031 (4) 0.030 (4) 0.024 (3) −0.020 (3) −0.007 (3) 0.003 (3)
O2 0.018 (3) 0.020 (3) 0.018 (3) −0.008 (3) 0.002 (2) −0.001 (2)
N11 0.017 (2) 0.017 (2) 0.014 (2) −0.0080 (16) −0.0034 (16) 0.0051 (16)
N12 0.020 (4) 0.020 (4) 0.014 (3) −0.011 (3) −0.001 (3) 0.000 (3)
C101 0.031 (5) 0.018 (4) 0.012 (4) −0.015 (4) 0.000 (4) −0.002 (3)
C102 0.023 (5) 0.031 (5) 0.012 (4) −0.012 (4) 0.003 (3) 0.000 (4)
C103 0.025 (5) 0.022 (5) 0.006 (4) −0.007 (4) −0.007 (3) 0.001 (3)
C104 0.026 (5) 0.021 (5) 0.019 (4) −0.011 (4) 0.003 (4) −0.002 (4)
C105 0.025 (5) 0.031 (5) 0.015 (4) −0.015 (4) 0.002 (4) 0.003 (4)
C106 0.024 (5) 0.022 (5) 0.013 (4) −0.001 (4) −0.001 (3) 0.001 (4)
C107 0.025 (5) 0.013 (4) 0.014 (4) 0.001 (4) 0.001 (3) −0.003 (3)
C108 0.032 (5) 0.024 (5) 0.017 (5) −0.010 (4) 0.000 (4) 0.001 (4)
C109 0.032 (5) 0.021 (5) 0.011 (4) −0.008 (4) 0.005 (4) −0.003 (3)
C110 0.039 (6) 0.027 (5) 0.008 (4) −0.004 (4) −0.002 (4) 0.000 (4)
C111 0.036 (5) 0.019 (4) 0.006 (4) −0.006 (4) 0.004 (4) 0.000 (3)
C112 0.026 (5) 0.024 (5) 0.017 (4) −0.008 (4) −0.001 (4) −0.002 (4)
C113 0.017 (4) 0.016 (4) 0.016 (4) −0.001 (4) −0.004 (3) 0.001 (3)
C114 0.021 (5) 0.028 (5) 0.018 (4) −0.016 (4) −0.003 (4) −0.001 (4)
C115 0.026 (5) 0.024 (5) 0.014 (4) −0.010 (4) −0.006 (4) 0.001 (4)
N21 0.023 (4) 0.029 (4) 0.008 (3) −0.014 (3) 0.002 (3) 0.003 (3)
N22 0.012 (2) 0.012 (2) 0.009 (2) −0.0042 (16) 0.0046 (16) −0.0034 (16)
C201 0.028 (5) 0.026 (5) 0.010 (4) −0.007 (4) 0.000 (3) −0.001 (4)
C202 0.029 (5) 0.031 (5) 0.015 (4) −0.008 (4) 0.001 (4) −0.001 (4)
C203 0.029 (5) 0.036 (6) 0.015 (4) −0.019 (4) 0.002 (4) −0.004 (4)
C204 0.045 (6) 0.019 (5) 0.022 (5) −0.016 (4) −0.006 (4) −0.001 (4)
C205 0.042 (6) 0.025 (5) 0.022 (5) −0.018 (5) −0.007 (4) 0.002 (4)
C206 0.033 (6) 0.045 (6) 0.016 (5) −0.018 (5) −0.006 (4) 0.000 (4)
C207 0.022 (5) 0.045 (6) 0.015 (4) −0.014 (5) −0.002 (4) 0.000 (4)
C208 0.023 (5) 0.035 (5) 0.008 (4) −0.009 (4) 0.000 (3) 0.003 (4)
C209 0.023 (5) 0.020 (5) 0.013 (4) −0.007 (4) −0.005 (3) 0.009 (3)
C210 0.021 (5) 0.025 (5) 0.012 (4) −0.004 (4) 0.000 (3) 0.000 (4)
C211 0.019 (5) 0.025 (5) 0.004 (4) −0.006 (4) −0.001 (3) −0.004 (3)
C212 0.013 (4) 0.025 (5) 0.017 (4) −0.003 (4) 0.001 (3) −0.004 (4)
C213 0.020 (5) 0.017 (4) 0.013 (4) −0.006 (4) 0.004 (3) −0.001 (3)
C214 0.018 (4) 0.023 (5) 0.015 (4) −0.008 (4) 0.001 (3) 0.000 (3)
C215 0.026 (5) 0.021 (5) 0.010 (4) −0.010 (4) 0.003 (3) 0.002 (3)
N31 0.026 (5) 0.038 (5) 0.034 (5) −0.015 (4) 0.002 (4) −0.008 (4)
N32 0.033 (5) 0.042 (5) 0.031 (5) −0.018 (4) −0.005 (4) 0.010 (4)
C301 0.032 (6) 0.025 (5) 0.040 (6) −0.019 (4) 0.003 (4) −0.005 (4)
C302 0.026 (5) 0.031 (5) 0.019 (5) −0.008 (4) −0.006 (4) 0.005 (4)
C303 0.019 (4) 0.025 (5) 0.007 (4) −0.013 (4) −0.005 (3) 0.002 (3)
C304 0.021 (4) 0.024 (4) 0.016 (4) −0.010 (3) −0.007 (3) 0.010 (3)
C305 0.028 (5) 0.045 (6) 0.013 (4) −0.020 (5) 0.002 (4) −0.008 (4)
C306 0.040 (6) 0.019 (5) 0.028 (5) −0.016 (4) −0.007 (4) 0.007 (4)
C307 0.026 (5) 0.024 (5) 0.030 (5) −0.005 (4) −0.007 (4) −0.007 (4)
C308 0.025 (5) 0.039 (6) 0.032 (5) −0.007 (5) −0.006 (4) −0.012 (5)
C309 0.032 (5) 0.035 (5) 0.016 (4) −0.012 (4) −0.001 (4) −0.003 (4)
C310 0.040 (6) 0.032 (5) 0.030 (5) −0.020 (5) −0.007 (4) 0.003 (4)
C311 0.021 (5) 0.023 (5) 0.024 (5) −0.016 (4) 0.007 (4) 0.002 (4)
C312 0.031 (6) 0.022 (5) 0.042 (6) −0.014 (4) −0.006 (5) −0.002 (4)
C313 0.028 (6) 0.024 (5) 0.057 (7) −0.007 (4) 0.010 (5) 0.012 (5)
C314 0.043 (6) 0.020 (5) 0.021 (5) −0.021 (5) −0.007 (4) −0.001 (4)
C315 0.024 (4) 0.018 (4) 0.028 (4) −0.009 (3) −0.005 (3) 0.012 (3)
Cl1 0.0150 (11) 0.0345 (13) 0.0266 (12) −0.0066 (10) 0.0037 (9) −0.0067 (10)
O3 0.016 (3) 0.035 (4) 0.031 (4) −0.003 (3) 0.013 (3) −0.003 (3)
O4 0.029 (4) 0.047 (5) 0.044 (4) 0.005 (3) −0.012 (3) −0.002 (4)
O5 0.048 (5) 0.066 (5) 0.029 (4) −0.041 (4) 0.015 (3) −0.010 (3)
O6 0.028 (4) 0.042 (4) 0.043 (4) −0.013 (3) −0.003 (3) −0.023 (3)
Cl2 0.0286 (13) 0.0232 (12) 0.0387 (14) −0.0086 (10) −0.0094 (10) 0.0107 (10)
O7 0.049 (5) 0.028 (4) 0.055 (5) −0.024 (3) −0.012 (4) 0.023 (3)
O8 0.055 (5) 0.051 (5) 0.061 (5) −0.026 (4) −0.024 (4) 0.043 (4)
O9 0.046 (5) 0.067 (6) 0.070 (6) −0.005 (4) 0.005 (4) −0.036 (5)
O10 0.024 (4) 0.028 (4) 0.056 (5) −0.010 (3) −0.010 (3) 0.000 (3)
C1 0.046 (7) 0.061 (8) 0.028 (6) −0.016 (6) −0.001 (5) −0.001 (5)
C2 0.064 (8) 0.045 (7) 0.029 (6) −0.003 (6) −0.005 (5) −0.003 (5)
O11 0.117 (8) 0.044 (5) 0.043 (5) 0.005 (5) −0.003 (5) 0.001 (4)