| Crystal data |
| Chemical formula |
[Cd(C15H18N2)2(H2O)2](ClO4)2·C15H18N2·C2H6O |
|
M
r
|
1072.34 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
120 |
|
a, b, c (Å) |
10.0618 (3), 10.1653 (3), 27.0304 (11) |
| α, β, γ (°) |
87.163 (1), 85.001 (1), 66.509 (1) |
|
V (Å3) |
2525.60 (15) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.60 |
| Crystal size (mm) |
0.10 × 0.07 × 0.05 |
| |
| Data collection |
| Diffractometer |
Nonius KappaCCD |
| Absorption correction |
Multi-scan (SADABS; Sheldrick, 2001 ▶) |
|
T
min, T
max
|
0.942, 0.971 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
20841, 9645, 6116 |
|
R
int
|
0.135 |
| (sin θ/λ)max (Å−1) |
0.617 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.091, 0.221, 1.10 |
| No. of reflections |
9645 |
| No. of parameters |
608 |
| No. of restraints |
24 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
2.94, −1.34 |
