| Crystal data |
| Chemical formula |
[Cu(C3H5NS2)(C6H8N2S3)]NO3
|
|
M
r
|
449.13 |
| Crystal system, space group |
Monoclinic, P21/m
|
| Temperature (K) |
293 |
|
a, b, c (Å) |
9.8937 (6), 6.9932 (5), 11.8054 (7) |
| β (°) |
102.078 (1) |
|
V (Å3) |
798.72 (9) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
2.04 |
| Crystal size (mm) |
0.35 × 0.12 × 0.06 |
| |
| Data collection |
| Diffractometer |
Bruker APEX CCD area detector |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2003 ▶) |
|
T
min, T
max
|
0.814, 1.000 |
| No. of measured, independent and observed [I > 2s(I)] reflections |
8700, 1534, 1402 |
|
R
int
|
0.026 |
| (sin θ/λ)max (Å−1) |
0.595 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.029, 0.080, 1.07 |
| No. of reflections |
1534 |
| No. of parameters |
133 |
| No. of restraints |
1 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.37, −0.27 |
