| Bruker SMART APEXII CCD diffractometer | 4776 independent reflections |
| Radiation source: fine-focus sealed tube | 3205 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.029 |
| ω and φ scans | θmax = 28.3°, θmin = 2.1° |
| Absorption correction: multi-scan (SADABS; Bruker, 2008) | h = −12→10 |
| Tmin = 0.662, Tmax = 0.746 | k = −13→14 |
| 18382 measured reflections | l = −25→25 |
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