| Bruker Kappa APEXII CCD diffractometer | 5367 independent reflections |
| Radiation source: fine-focus sealed tube | 3097 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.034 |
| ω & φ scans | θmax = 28.3°, θmin = 2.0° |
| Absorption correction: multi-scan (SADABS; Bruker, 2008) | h = −14→14 |
| Tmin = 0.977, Tmax = 0.985 | k = −16→16 |
| 37978 measured reflections | l = −21→19 |