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. 2014 Jul 31;70(Pt 8):o883. doi: 10.1107/S1600536814016638
Bruker Kappa APEXII CCD diffractometer 5367 independent reflections
Radiation source: fine-focus sealed tube 3097 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.034
ω & φ scans θmax = 28.3°, θmin = 2.0°
Absorption correction: multi-scan (SADABS; Bruker, 2008) h = −14→14
Tmin = 0.977, Tmax = 0.985 k = −16→16
37978 measured reflections l = −21→19