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Initial radiofluorination of precursor 15 & 16 using microfluidics.
| ||||
|---|---|---|---|---|
| Run | X | Temp (°C) | Transfer Rate (μl) | RCY (%) |
| 1 | Cl | 140 | 40 | 0 |
| 2 | Cl | 160 | 40 | 0 |
| 3 | Cl | 180 | 14 | 5.2 |
| 4 | Br | 140 | 40 | 0 |
| 5 | Br | 160 | 40 | 1 |
| 6 | Br | 180 | 60 | 7 |
*Precursors 15 & 16 stable up to 180 °C.
