Table 1.
Zone | [100] | [110] | [110] | [111] | [120] | [120] | [123] | [123] | [210] | [210] | [211] | [221] | [311] | [311] |
---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Level | 0 | 0 | 1 | 0 | 0 | 1 | 0 | 1 | 0 | 1 | 0 | 0 | 0 | 2 |
Precession angle (°) | 2.0 | 2.0 | 1.5 | 2.0 | 2.0 | 1.5 | 2.0 | 1.5 | 2.0 | 1.5 | 2.0 | 2.0 | 2.0 | 1.5 |
Nunique ideal | 251 | 214 | 216 | 193 | 120 | 183 | 141 | 237 | 120 | 183 | 210 | 153 | 279 | 387 |
Nunique measured | 244 | 185 | 203 | 188 | 114 | 174 | 126 | 227 | 114 | 173 | 186 | 143 | 267 | 358 |
Overlaps | 107 | 107 | 159 | 106 | 85 | 147 | 111 | 208 | 89 | 142 | 149 | 114 | 195 | 299 |
Rfilm pack | 11.8 | 5.9 | 11.8 | 10.5 | 10.5 | 7.0 | 6.2 | 6.8 | 10.6 | 5.3 | 8.9 | 13.0 | 5.5 | 14.2 |
Rsym | 7.0 | 2.9 | 11.9 | 6.7 | 5.3 | 12.8 | 4.6 | 8.1 | 4.0 | 8.1 | 4.3 | 6.5 | 3.9 | 14.0 |
Rmerge | 7.2 | 4.8 | 13.7 | 5.5 | 4.6 | 7.5 | 3.5 | 6.5 | 4.2 | 7.0 | 8.7 | 6.3 | 3.7 | 12.4 |
Total unique reflections measured: 1481 out of 1567 total possible.
Overall R factor: 5.7% (1205 overlaps).