Figure 5.

(Solid line) Experimental 1D synchrotron SAXS profile of shear-oriented PDMA–PS monolith (sample A) at 25 °C and (dashed line) simulated form factor scattering curve generated for cylinders with an 11.3 nm radius (value extracted from the experimental SAXS profile). The black triangles indicate the expected reflections for a cylindrical morphology (√1; √3; √4; √7; √9; √12; √13; √16). Corresponding TEM images of the material, obtained (left) perpendicularly and (right) parallel to the shear direction (PS domains, appearing darker, were stained by RuO₄ vapors).