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. 2014 Sep 5;136(37):13016–13028. doi: 10.1021/ja506133z

Table 3. Enantioselective Sulfenylation of Various Silyl Enol Ethers.

6.

6.

a

Yield of isolated, analytically pure product. All reactions were carried out on a 1.0 mmol scale.

b

The enantiomeric ratio was determined by CSP-SFC analysis or CSP-HPLC analysis, as required.

c

10 mol % Lewis base was used in this instance.

d

% conversion determined by GC analysis using biphenyl as an internal standard.

e

After one recrystallization from MeOH.