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. 2014 Sep 23;16(19):5044–5047. doi: 10.1021/ol502389g

Table 2. Various Conditions of ReSET To Afford 3-6.

graphic file with name ol-2014-02389g_0008.jpg

entry scale (mg) time (min) T (°C) power (W) AcOH (equiv) 3 (%) 4 (%) 5 (%) 6 (%)
1 113 overnight rt no 3 4 11 20 43
2 207 30 60 30 3 5 13 22 24
3 234 30 70 40 2 11 20 17 28
4 470 18 58 30 2 13 8 32 46
5 196 45 55 30 1 28 31 16 11