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. 2014 Aug 30;70(Pt 9):153–156. doi: 10.1107/S1600536814019254

Table 2. Experimental details.

Crystal data
Chemical formula C14H17FN2O
M r 248.30
Crystal system, space group Monoclinic, P21/n
Temperature (K) 100
a, b, c (Å) 11.3414 (3), 9.1909 (3), 12.6799 (4)
β (°) 111.569 (2)
V3) 1229.17 (7)
Z 4
Radiation type Cu Kα
μ (mm−1) 0.79
Crystal size (mm) 0.23 × 0.22 × 0.21
 
Data collection
Diffractometer Bruker X8 Proteum
Absorption correction Multi-scan (SADABS; Bruker, 2013)
T min, T max 0.834, 0.848
No. of measured, independent and observed [I > 2σ(I)] reflections 8574, 2009, 1488
R int 0.071
(sin θ/λ)max−1) 0.585
 
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S 0.043, 0.122, 1.00
No. of reflections 2009
No. of parameters 168
H-atom treatment H atoms treated by a mixture of independent and constrained refinement
Δρmax, Δρmin (e Å−3) 0.20, −0.22

Computer programs: APEX2 and SAINT (Bruker, 2013), SHELXS97 and SHELXL97 (Sheldrick, 2008), PLATON (Spek, 2009), Mercury (Macrae et al., 2008) and publCIF (Westrip, 2010)’.